On Tuesday, we prepared the FROSTI for disassembly in anticipation of the APS filming that is set to take place in the labs. The FROSTI has been unbolted from the optical table in the cleanroom, with its wires weighted down and the majority of its screws removed to ensure an easy removal of the reflectors during the filming process. As of now, the new filming date is TBD.

Attached below are updated plots for the FROSTI RIN measurements for Jan 14 group meeting.

[Luke, Tyler, Cynthia, Shane, Michael]

Summary of Cleaning Activities:

We began cleaning Room 1119 at 2:00 PM.

At 2:30 PM, we moved to Room 1129 and continued cleaning.

Cleaning tasks included wiping down dust-collecting surfaces and vacuuming the floors.

Once the labs were clean, we proceeded to the cleanroom. 

• Wiping down surfaces and soft walls
• Vacuuming, mopping the floor, and finishing with IPA wipes

Particle Count Measurements:

• Pre-cleaning (2:30 PM):
  • Zone 3:
    • 0.3 µm: 973
    • 0.5 µm: 354
    • 1.0 µm: 132
  • Zone 4:
    • 0.3 µm: 486
    • 0.5 µm: 177
    • 1.0 µm: 0
• Post-cleaning (4:10 PM):
  • Zone 3:
    • 0.3 µm: 619
    • 0.5 µm: 132
    • 1.0 µm: 0
  • Zone 4:
    • 0.3 µm: 397
    • 0.5 µm: 0
    • 1.0 µm: 0

[Luis, Luke]

RGA Volume: T = 22°C, P = 2.10e-9 Torr
Main Volume: T = 21°C, P = 5.71e-9 Torr

Measurements of the current state of the vacuum systems were taken today, now that the system had reached UHV status, the results are attached bellow. The first plot overlays the data of the empty chamber taken on 12/16/24 before inserting the MR material, and the data of the system today, with the MR inside. The second plot displays the S/N Ratio of the system. The last plot displays the data of the system with the Ar leak open and closed. Notice that it is common for the Ar leak close data to fail due to the calculation of the gas flux per unit ion current, which is dependent on the Ar peak.

[Luis, Luke]

RGA Volume: T = 23°C, P = 3.0e-9 Torr
Main Volume: T = 22°C, P = 9.90e-9 Torr

After letting the vacuum cool down for a couple days, we reattached the magnets and sensors, then we performed a RGA scan of the vacuum system, now containing the MR sample. The results are attached below. Something to notice is that we are technically not under UHV, though Luke and I believe the reading of the sensor is not completely accurate since it was still coming to a steady state, further test will be performed when the physics building is open again.

The vacuum chamber has stopped baking. 

Current state as of 11:40, 12/19/2024:

The gate valve is open, and the filament of the RGA is on.

The temperatures were steady at:

PID right: barrel upper: 129°C,  RGA volume: 125°C

PID left: barrel lower: 125°C, Lid: 114°C

The RGA flange was 37°C

Cleanroom was 26°C

Note the upper barrel was very close to the emergency shut off temp of 130°C. In the future we may want to either rewire some of the heating tape or lower the set temperature of the right PID controller.

Luis and I are planning on taking an RGA scan of the MR on Sunday before the campus shuts down for the holidays.

I have begun the (hopefully) final RIN measurements at 3:30 PM today. If you need to go into the cleanroom at any time between now and Sunday (the 22nd), please do not touch the FROSTI, the Red Pitaya, the photodetectors, or any of the wiring.

[Luis]

The vacuum system is being baked. I disconnected the digital gages and the magnets, opened the Ar leak and started the bake by taking the temperature from 60C-90C-125C waiting about 15-20 minutes between each interval. The RGA electronics were left on since the temperature of the flange was 36.6C (bellow the 60C threshold)

[Luis, Luke]

The MR material was placed in the vacuum chamber following standard procedures to ensure the vacuum remained as clean as possible. During this process, we only opened the main volume while keeping the gate valve between the two volumes closed to maintain the UHV in the RGA section.

An RGA scan was taken before this process, this will be used to compare the state of the vacuum with the sample inside to determine whether the MR material is vacuum compatible.

[Luis]

RGA Volume: T = 23°C, P = 1.71e-9 Torr
Main Volume: T = 22°C, P = 5.71e-9 Torr

On 12/13 I took another RGA scan to verify the state of the vacuum system and to see whether the degassing of the filament had worked. The results of the scan shows that we did get an overall improvement of the noise levels, though we still have some peaks that are higher than the rest.

Also, while I was around, I transferred the Viton O-rings to a bag and labeled it properly. They are ready to be put into the clean room.

[Luis, Luke]

RGA Volume: T = 21°C, P = 1.74e-9 Torr
Main Volume: T = 22°C, P = 5.60e-9 Torr

We performed an RGA scan of the system. As we can see, we met cleanliness standards. The S/N ratio was roughly calculated and it is about 100. I will update the code to make this calculation and to have it displayed on the plot in the next scan we perform.

After this, we closed the RGA to the main volume valve, degassed the filament, and after the pressure came down to what it was initially, we reopened the valve. After the degassing, we took another scan. The overlaid plots are attached below.

The noise floor seemed to be about the same. I will take another scan tomorrow to verify whether it was the same or if the system just needed a little more time to be completely clean.

[Luis]

I rebooted Spica and I was able to connect the RGA again. After Connecting the RGA, I left the filament on.

Attached below are updated ASD plots for the FROSTI RIN measurements. The parameters set for this are the following:

• DFT Size (N): 16384
• Sampling Frequency (F_s): 7.629 kHz
• Resolution (F_s/N): 0.47
• CH0 DC Voltage w/FROSTI ON: 113.6 mV
• CH0 DC Voltage w/FROSTI OFF: -5.7 mV
• CH1 DC Voltage w/FROSTI ON: 113.0 mV
• CH1 DC Voltage w/FROSTI OFF: -5.7 mV

Each measurement was recorded over a roughly two-day period. Before each spectrum was computed, the time-series signals were AC-coupled (i.e. the DC offset was subtracted from the data). The low-pass filters are still attached for dark and light noise measurements. ADC noise is measured with two 50-ohm terminators attached to the Red Pitaya inputs rather than the IR photodetectors.

[Luis,Shane]

An RGA scan was taken on Dec 4th. The results are attached at the end of the e-log. As we can see, the scan results are under the allowed limits. After the scan, Shane and I worked on the vacuum connections. The filament was turned off, and the RGA was disconnected from Spica.

After we finished the tests, we reconnected the RGA and attempted to turn the filament back on. However, the program was unable to connect to the instrument. We checked for any loose connections but did not find anything. The RGA connection needs to be troubleshot and fixed.

[Luke, Luis]

We couldn't access the bake log on the wiki. (see attached) So we looked in the documentation provided on the DCC to find at what temperature to bake the Viton O-rings. We found that we should bake Viton at 180°C for 24 hours. 

So we sonic-washed the O-rings, dried them, and then put them in the oven set to the following:

100°C in 15 minutes

100°C for 30 minutes

180°C in 30 minutes

180°C for 24 hours

30°C in 2 hours

Other things of note:

We refilled the water container as it was running out.

The nitrogen used to dry the clean and baked objects is now critically low.

The helium used in leak testing is also quite low (~400 psi).

Regarding the vacuum chamber:

I reattached the pressure gauges to the chamber and gave them about an hour to stabilize. They read out main 8.7e-9, RGA 2.6e-9. Please note these pressures should lower more as we only stopped baking on Saturday afternoon. 

Update Slides

The vacuum chamber has stopped bakeing. 

Current state as of 12:10, 11/30/2024:

The gate valve is open, and the filament of the RGA is on.

The temperatures were steady at:

PID right: barrel upper: 128°C,  RGA volume: 125°C

PID left: barrel lower: 125°C, Lid: 113°C

The RGA flange was 38°C

Cleanroom was 26°C

[Luke, Luis]

The vacuum chamber is currently baking. 

We stepped up to 125°C by increments of 30°C starting at 60°C. Everything went fine. After about 20 minutes of the PID controllers being set to 125°C, the flange closest to the RGA was 38°C, so we left it connected. 

Current state as of 4:15:

The gate valve is open, and the filament of the RGA is on.

The temperatures are as follows:

PID right barrel upper: 105°C,  RGA volume: 125°C

PID left barrel lower: 125°C, Lid: 82°C

The lower temperatures should climb as the whole system heats up. 

I will come in Saturday afternoon to turn them off so that we can look at the pressures on Monday. 

I downgraded the Red Pitaya back to OS 2.00-18 due to runtime errors during measurement. Once I did this, the device appeared to work much better than it has the last few weeks. First, it appears we can actually see the cutoff of the added low-pass filters that were added in to the RIN setup. Second, there does appear to be a difference again between the FROSTI ON state versus the dark state (i.e. FROSTI OFF). A long measurement of the ADC noise floor in the current configuration still needs to be recorded, but it does appear that the recent highlighted issues with the Red Pitaya have been solved.

[Luke, Luis]

Update of current state of vacuum chamber

Current temp: 24°C

Current pressure: Main 1.77e-8, RGA 5.3e-9 [torr] (Gate valve open)

Summary of recent work-->

To try and reduce the leak in the turbo pump by reducing cross-connection, we replaced the copper gasket. This made no improvement to the leaks.

Initially: 1.9e-9 --->

Left side: 1.33e-9, Right side: 3.37e-9 (Gate valve open)

This is still a significant leak. We have tried to tighten the bolts further, but they are as tight as reasonably possible. 

Things of note: While examining the knife edges, we found some very slight imperfections on the reducing cross's flange as seen in 474. This could be the source of our leak. We have replaced this gasket 1-2 times already and consistently have a slight leak. This imperfection is on the right side of the flange, which would be consistent with the measurements above. 

Unless we want to use the liquid sealant or replace the gasket with an annealed gasket, we could try baking the system again, as this allowed us to reach UHV in the main volume before. It also allowed us to pass the RGA scan, which we are currently failing. (see attached)

[Luke, Luis]

After the gasket replacement performed on Monday (11/18/24) we let the vacuum pump down to UHV pressure for a couple days. Today (11/20/24) we measured the pressure to be 5.30*e^-9 with a temperature of 22C, and we performed a leak test and RGA Scan.

Here are the results:

Chamber temperature: 23C

Chamber Initial Pressure: ~1.8e-8 main, ~3.5e-8 rga

Did another leak test after monday's work to check how the seal was holding up initial leak was 5.5e-9. I then tried to tighten the bolts a bit more the leak rose to 1.9e-8 about a factor of 4 change.

I checked another flange to confirm that I was preforming the test properly. I measured the elbow to pressure sensor to be 2.2e-11 aproximatly what it was earlier in the month (1.9e-11). 

I ran another isolation test. It is still exponetial. Graph attached.

Thoughts:

I belive at this point that it is a knife edge issue when replacing the gasket I checked both flanges and the new gasket. The tp knife edge seemed perfectly fine, the gasket had very minor scratches, and the reducing cross had very small imperfections on its edge. 

We may want to try and use the liquid sealant or get annealed gaskets for 4.5"

[Luke, Luis, Michael]

cleaning cleanroom and particle count

• 8:30 am: started particle count
  • zone 3:
    • 0.3 u: 1195
    • 0.5 u: 177
    • 1.0 u: 132
• zone 4:
  • 0.3 u: 619
  • 0.5 u: 0
  • 1.0 u: 0
• 9:00 am: began surface check and wipedown, including softwalls
• 9:35 am: started vacuuming the floor
• 9:43 am: finished vacuuming the floor
• 9:45 am: started mopping the floor
• 9:55 am: finished mopping the floor
• 9:56 am: started cleaning the buckets
• 10:00 am: started mopping with IPA wipes
• 10:05 am: finished mopping with IPA wipes
• 10:20m: started particle count
  • zone 3:
    • 0.3 u: 2213
    • 0.5 u: 398
    • 1.0 u: 0
• zone 4:
  • 0.3 u: 1150
  • 0.5 u: 177
  • 1.0 u: 44

slides

We've added two low-pass filters in hopes of reducing any potential aliasing that may be introducing additional noise into the power spectra for the RIN measurements. It still looks like the noise levels are too high. Attached below are some recent measurements taken with the FROSTI powered on and off.

[Luis, Luke, Ma Michael]

The isolation test was conducted on the vacuum system. Every pump was turned off under vacuum, and pressure measurements were taken every minute for 15 minutes. The results are displayed in the sheet linked at the end of this report. The pressure of the main volume dropped very slowly.

The pressure of the RGA Volume dropped in an exponential manner. The test had to be paused at 11 minutes due to concerns about the pressure exceeding the lowest permitted level for the RGA filament.

After the ISO test was performed, we attempted to tighten the bolts of the small turbo pump on the RGA Volume. However, we noticed that the pressure had increased by nearly an order of magnitude, going from 3.27 × 10^-9 Torr to 1.45 × 10^-8 Torr when both volumes were separated. We conducted a leak test for that particular flange and found a concerning leak of 2.15 × 10^-8 Torr, which had previously been 1.9 × 10^-9 Torr. We believe the copper seal was damaged during the ISO test.

View the results sheet

[Luke, Luis]

On Friday, 11/1/24, the MR was unpackaged and cleaned under the flow bench. We noticed an ink stain on one of the corners of the material. After wiping it down with IPA and Vector Alpha wipes, the stain was removed. However, the material showed some wear.

After cleaning, we placed it in the bake station and applied a stainless steel baking protocol. On Tuesday, 11/4/24, the material was removed from the furnace and packaged in a static shielding bag. The MR was wrapped in Vector Alpha wipes.

The Red Pitaya ecosystem has been upgraded to OS 2.00-35, with a key feature being greater freedom in adjusting the sampling frequency for signal analysis. Before, decimation factors could only be applied if they were a power of 2 (i.e 2,4,8,16,...) up to 65536. Now, the factors can be any power of two up to 16, and any whole number greater than 16 up to 65536. Further information can be found here.

We replaced the 1A breaker in the timing chassis today with a 4A one, and tested that all is working well. The chassis successfully outputted the correct signal (image attached). The real time models have also been restarted and the CyMAC diagnostics screen is showing all green flags. Timing chassis has been closed up and reinstalled in the server rack.

PowerPoint slides new

PowerPoint slides older

[Luke, Luis, Mary, Ma]

On 10/22/24 Luke, Ma, Mary and myself ran a RGA scan, the results are displayed below. The overall pressure of the vacuum was 2.0e-8 and the temperature readings were 26C for the RGA and 25C for the main volume.

As we can see, the vacuum is passing cleanliness standards again.

[Luke, Luis, Mary, Ma]

On 10/22/24 Luke, Ma, Mary and myself ran a leak test, the results are displayed below. The overall pressure of the vacuum was 2.0e-8 and the temperature readings were 26C for the RGA and 25C for the main volume.

[Ma, Luis, Shane]

Working theory for the timing chassis issues had been that the 1A breaker was tripping and causing the failure of the Valon 5015 and 3010 to output the timing signal correctly. We just tried bypassing the breaker, running 6 V on the benchtop power supply (set the current limit to 1.5A), with the 5010 generating the sine wave to pass to the 3010. All worked correctly, and there were no issues. Square wave outputted by the 3010 was exactly as desired (image attached) at the correct frequency, and this confirms the issue was the breaker, not the valon 5015. Ready to go ahead with ordering a new replacement breaker.

The following figure displays data acquired on 10/09, and it shows that we are no longer below the cleanliness standard. Also, the system's pressure went up to 1.9x10^-8 Torr (approximately 7x10^-9 Torr previously). This might be due to a leak somewhere in the system. More tests will be performed later.

I conducted separate tests on the '5015' and '3010a'. When powered individually, the '5015' outputs a signal at 33.55 MHz with an amplitude of 608 mV. It draws 1 A of current from the power source. The input signal for the '3010a' is 33.54 MHz with an amplitude of 670 mV (peak-to-peak) and a 15 mV DC offset. The output signal from channel 1 is a 65.5 kHz square wave with an amplitude of 3.28 V. The '3010a' draws 0.1 A of current.

Both the '5015' and '3010a' work fine when powered separately. However, when both are powered together, the power source behaves as if there is a short circuit. The current theory is that the switch or breaker is tripping, as it has a 1 A current rating. Since the combined current demand of both devices exceeds 1 A, this may be causing the issue.

Slides for 10/16/2024 Group Meeting

I tried adjusting the gain settings on the photodetectors to check if this would help improve the RIN spectra measurements. Overall, it doesn't look like it does, and if anything, looks worse. I assume this is so because as the gain is lowered, the amount of detectable signal from the FROSTI becomes smaller and smaller.

cleaning cleanroom and particle count

• 12:25 pm: started particle count
  • zone 3:
    • 0.3 u: 4614
    • 0.5 u: 872
    • 1.0 u:83
• zone 4:
  • 0.3 u: 2411
  • 0.5 u: 415
  • 1.0 u: 83
• 12:48 pm: began surface check and wipedown, including softwalls
• 1:20 pm: started vacuuming the floor
• 1:30 pm: finished vacuuming the floor
• 1:34 pm: started mopping the floor
• 1:40 pm: finished mopping the floor
• 1:40 pm: started cleaning the buckets
• 1:42 pm: started mopping with IPA wipes
• 1:50 pm: finished mopping with IPA wipes
• 1:51 pm: changed sticky floor mats
• 3:44 pm: started particle count
  • zone 3:
    • 0.3 u: 3207
    • 0.5 u: 624
    • 1.0 u: 83
• zone 4:
  • 0.3 u: 916
  • 0.5 u: 83
  • 1.0 u: 0

Power point slides

Group Meeting slides for Non-deterministic Heater Response.

The following images compare the RGA scans from 9/23/24, after the first bake with the new vacuum system, with those from 3/14/24, after bake 12 with the old system.

The first image shows a graph of the raw data and includes the calibrated leak for both curves. As we can see, our new system meets LIGO standards of cleanliness.

The second graph contains the plot of the normalized data.