ligo-ex ligo-ds
  Richardson Lab Experimental Log, Page 7 of 10  Not logged in ELOG logo
ID Datedown Author Type Category Subject
  170   Mon Jul 24 14:55:53 2023 JonUpdateVACRemoved extension power cable
I removed the extension cable that was powering the leftmost heater controller, since there is no bake currently happening. It is currently powering the LED over the electronics bench, and can be removed if needed. I will be ordering more extension cords to permanentize our setups.
  169   Thu Jul 20 21:00:23 2023 PamellaUpdateFLIRData plot FLIR and updates about the black body
[Pamella]
  • Today I got more data to plot the Gaussian. So I took more snaps in each position for the six different spots than we be using to have a better calibration of the FLIR collected data. I attached the new plot below. Also, I did the same plot for each region as on the Elog 167 but I have more than 20 pics because I was using a big number of data so I just attached one example below.
  • To access the Elog, click here.

  • Also I think we have some real (non-ideal) heat diffusion by the screen and not noise like Dr. Richardson suggested. I was testing today and we can see the first pic before the start heater source turns on, the second pic is at 120.2 C (0.31A) with the heater on and the last pic is after the heater source cooled back down to room temperature. Just in the second pic, we have a strong spot on the top, so it looks like a non-ideal diffusion.
  168   Thu Jul 20 18:03:19 2023 AidenUpdateVACVacuum Chamber Baking Update

Took another set of RGA data after the second bake has cooled down to 27 degC.

Just by visual comparison to the other graphs, the HC levels of the chamber has gone down further. I will soon overlay the data for an easier comparison.

I also reinstalled the full range gauge above the RGA line. It is still adjusting itself downwards so I will have to check again to get an accurate measurement of the pressure.

  167   Wed Jul 19 19:10:31 2023 PamellaUpdateFLIRData plot FLIR and updates.
[Pamella]
  • Today I was able to plot a graph for the isolation point on the center of the heater. I got data from six different positions on the screen (I shifted the all coordinates). I extracted the data for the center point and plot the Gaussian with this extracted data for temperature. I attached the all plots below
  • Also I took a snap using the black wall and with the heater at 120.1 C (0.30 A) try to have less noise but we can see this is not very good. At this temperature, we have noise on the top and I don't understand why because the heater is not in this location. I attached a snap below.
  166   Wed Jul 19 14:39:19 2023 Pamella, Shane, AidenUpdateCleanroomcleaning and particle count
[Pamella, Shane, Aiden]

cleaning cleanroom and particle count

  • 1:10 pm: started particle count
    • Zone 3:
        0.3 u: 2535
        0.5 u: 207
        1.0 u: 41
    • Zone 4:
        0.3 u: 789
        0.5 u: 41
        1.0 u: 0
  • 1:30 pm: began surface check and wipedown
  • 1:41 pm: started vacuuming the floor
  • 1:55 pm: finished vacuuming the floor
  • 1:57 pm: started mopping the floor
  • 2:01 pm: finished mopping the floor
  • 2:02 pm: started cleaning the buckets
  • 2:08 pm: started mopping with IPA wipes
  • 2:17 pm: finished mopping with IPA wipes
  • 2:18 pm: changed sticky floor mats
  • 2:19 pm: started particle count
    • Zone 3:
        0.3 u: 3990
        0.5 u: 1080
        1.0 u: 374
    • Zone 4:
        0.3 u: 540
        0.5 u: 207
        1.0 u: 0
  165   Tue Jul 18 16:35:06 2023 PamellaUpdateFLIRPlot-Data with the new configuration without the mask and reflector.
[Pamella]
  • I was able to plot the first graph for a result between the six different positions on the screen, for now we can see the behavior of the heater temperature in a Gaussian graph with combination data between the six files.
  • To do: Tyler gave me some ideas today to improve the plot. So I'm going to change the code to have insulation on the values for just the heater ("insulation") and I'm going to plot after this insulation data as well I'm going to get more data and compare with more data for the same position.
  • I was using the data than I got last week and I shared on Elog (151) and we can see on this quote

Quote:
[Pamella] I started collecting data by moving the camera FLIR and covering all six positions on the screen (2x3). I was looking and taking snaps for more than one hour and a half. I'll repeat this one more time to make sure we have enough data to do analysis. I attached snap data below. This images is processed on python code.

 

  164   Tue Jul 18 16:12:27 2023 PamellaUpdateFLIRThermocouple plot.
  • I noticed that these measurements have some issues with the weather on different days. We can see in the photo attached below how different the temperatures are on different days, I took the data with the same procedure every day, but we can see the differences between them.
  • To Do: I will do a new data collection using FLIR and thermocouple at the same time to plot comparison between both.

Quote:
[Pamella]
  • I collected data to plot a calibration with the heater. I took measurements with current and temperature (the thermocouple - thermometer) to compare with the FLIR measurements.
  • I made a plot with this data and we can see how temperature vs current behaves. Note: This data I measured manually.

 

  163   Tue Jul 18 16:04:26 2023 PamellaUpdateFLIRSetup FLIR with black wall (black body)
[Pamella]
  • Today I tried get data the heater with the black screen but doesn't looks possible have just one "energy" point straight to FLIR camera. Tyler and I tried different current and temperatures but keep very bad data. I attached a snap below.
  • I attached a photo about the new setup below. The FLIR is in the most close point possible/safety with the heater. The heater is very close to the black wall but is not touch the screen so is safety.
  162   Tue Jul 18 14:13:46 2023 Sophia UpdateScripts/ProgramsUpdate on Laser Noise Data Collection and Analysis
We [Sophia and Tyler] have found a code which will partition our data and generate PSD's and CSD's automatically. We are now in the stage of writing this into a dynamic code, which so far has been fast-paced because of the framework we have built for it over the past few weeks. Something to note is that we have found, especially over long periods of time, the laser goes through periods of extreme noise and the signals often cross from where we set them at some point throughout our data collection. We have made the assumption that this is something to do with the laser itself, and not our setup or surrounding space because of both the times that these noise/intensity spikes took place and the duration of the spikes (1.5-2.5 hours). To try and correct for this, we have been "cutting" the noise, and just looking at sections which don't include these big fluctuations. An example of the "noise cut data" is shown in the graph titled "Signals Over Time 7-18-23 Noise Cut Data" and all of the PSD/CSD graphs have been made using only these "noise cut" regions.
  161   Mon Jul 17 14:01:41 2023 AidenUpdateVACVAC System Heating Update

The insulation on the lid of the vacuum chamber has some discoloration and it may be wise to place a sensor closer to this spot in future bakes.

  160   Mon Jul 17 13:50:41 2023 AidenUpdateVACVAC System Heating Update

Started to cool down the chamber today. Final temperature readings of the chamber were 146C and 91C for the body and cross respectively.

  159   Mon Jul 17 11:46:24 2023 PamellaUpdateFLIRThermocouple plot.
[Pamella]
  • I collected data to plot a calibration with the heater. I took measurements with current and temperature (the thermocouple - thermometer) to compare with the FLIR measurements.
  • I made a plot with this data and we can see how temperature vs current behaves. Note: This data I measured manually.
  158   Sun Jul 16 15:21:56 2023 PamellaUpdateGeneralGeneral update about some problems in the lab.
[Pamella]
    General information about the lab facility.
    1. Changed sticky floor mats, because close to entrance the cleanroom, both sticky floor had a many died ants on top.
    2. The light on top of the internet cable bridge is burned out.. I just saw this today but I am not sure if was like this before.
    3. The ant bait traps seem very efficient and right now only a few ants are running around in the lab, most are dead in the bait traps, so probably in a day or two we can change those bait traps.
  157   Fri Jul 14 16:49:42 2023 PamellaUpdateFLIRNew bridge and calibration data
[Pamella]
    Aiden 3D printed a new bridge for the heater and I installed the new bridge yesterday.
    I started collecting data to plot a calibration with the heater. I'm doing measurements with current and the thermocouple (thermometer) to compare with FLIR measurements and have a good calibration.
  156   Fri Jul 14 14:37:25 2023 AidenUpdateVACVAC System Heating Update

Checked on the vacuum system and it looks like it will either need to be increased in temperature or baked for a longer time. The main body is at 146C while the cross is at 91C.

  155   Thu Jul 13 16:59:03 2023 JonUpdateGeneralAnt traps placed around lab

Update: After seeing the strong response to the first set, I redistributed them to the hottest spots and added one more trap.

Quote:

In response to reports that ants have been observed in the lab, I placed five ant bait traps around the room today. Each is sitting on the floor on top of a piece of aluminum foil, in areas unlikely to be inadvertently stepped on. They contain liquid which will spill out if picked up, so please take care not to disturb them.

 

  154   Thu Jul 13 15:31:21 2023 JonUpdateGeneralAnt traps placed around lab

In response to reports that ants have been observed in the lab, I placed five ant bait traps around the room today. Each is sitting on the floor on top of a piece of aluminum foil, in areas unlikely to be inadvertently stepped on. They contain liquid which will spill out if picked up, so please take care not to disturb them.

  153   Thu Jul 13 14:56:43 2023 AidenUpdateVACVAC System Heating Update

Checked on the vacuum system today to change the PID controls back to their default values in order to try and get the temperature of the cross in front of the turbo pump higher. Currently it is sitting at 90 degC before changing the controls. While the main body is at 146 degC.

Will update again tomorrow on new equilibrium with the default PID settings.

  152   Mon Jul 10 13:23:23 2023 AidenUpdateVACVAC System Heating Update

Checked on the system today.

The flange on the turbo pump has reached an equilibrium temperature of 87 degC when set at 150 degC. While the main body of the chamber has reached an equilibrium temperature of 142 degC.

  151   Sat Jul 8 14:26:17 2023 PamellaUpdateFLIRData with the new configuration without the mask and reflector.
[Pamella] I started collecting data by moving the camera FLIR and covering all six positions on the screen (2x3). I was looking and taking snaps for more than one hour and a half. I'll repeat this one more time to make sure we have enough data to do analysis. I attached snap data below. This images is processed on python code.
  150   Fri Jul 7 15:11:39 2023 AidenUpdateVACVAC System Heating Update

The temperature of the flange connecting to the turbo pump after reaching equilibrium is 74 degC. This means that it is safe to proceed with raising the temperature from 120 degC to 150 degC.

Raised the set temperature of the chamber from 120 degC to 150 degC in 15 deg steps.

  149   Thu Jul 6 18:03:19 2023 PamellaUpdateFLIRFLIR project - New configuration
[Pamella]
    Cao suggested using the project without the reflector and mask because in this case we probably got good images around the screen. So I started this yesterday and today I started to get some data to see the stabilization position and check how the parameters fluctuated. I was looking and taking snaps for an hour and a half. I'll repeat this one more time to make sure we have enough data to do analysis.
    To do: The next step is to start collecting data by moving the camera FLIR and covering all six positions on the screen (2x3). Also Aiden is on hand to help and is going to make a new 3D print bridge to have good heater support.
    I attached a image for the new configuration below and a snap data.
  148   Thu Jul 6 16:16:03 2023 AidenSummaryVACVacuum Chamber Baking Update

Pressure Measured Before Removing Gauge 2.31 E-7 Torr.

Went in and turned on the heating tape in increments of 30 degC until 120 degC was reached. I will let it equilibrate over night and then asses whether or not the chamber can be raised to 150 degC without having the flange to the turbo pump reach over 120 degC as it is not recommended for that flange to be any hotter.

If it can safely be raised to 150 degC, then only 2 days of baking is necessary. If 120 degC is the bake temperature, a week will be needed.

  147   Thu Jul 6 13:34:48 2023 Pamella, Shane, Julian, AidenUpdateCleanroomcleaning and particle count
[Pamella, Julian, Aiden, and Shane]

    cleaning cleanroom and particle count

  • 12:00 pm: started particle count
    • Zone 3:
        0.3 u: 2826
        0.5 u: 457
        1.0 u: 166
    • Zone 4:
        0.3 u: 457
        0.5 u: 83
        1.0 u: 41
  • 12:17 pm: began surface check and wipedown. NOTE: found a few ants crawling up the metal table frame and on the desk
  • 12:29 pm: started vacuuming the floor
  • 12:45 pm: Finished vacuuming the floor
  • 12:46 pm: Started mopping the floor
  • 12:52 pm: Finished mopping the floor
  • 12:55 pm: Started cleaning the buckets
  • 1:02 pm: Started mopping with IPA wipes
  • 1:11 pm: Finished mopping with IPA wipes
  • 1:12 pm: Changed sticky floor mats
  • 1:14 pm: started particle count
    • Zone 3:
        0.3 u: 2577
        0.5 u: 457
        1.0 u: 166
    • Zone 4:
        0.3 u: 457
        0.5 u: 41
        1.0 u: 0
  146   Wed Jul 5 16:02:12 2023 AidenUpdateClean & BakeClean and Bake batch 14 Bagging
Bagged and Tagged the 2.75" copper gaskets from Batch 14 and placed them into the clean room on the work bench.
  145   Wed Jul 5 15:46:47 2023 Aiden, CaoInfrastructureVACVacuum Chamber Baking Update

Cao and Aiden put the RGA back on to the chamber and measured the outgassing rate after the chamber has cooled down from its first bake. The figure attached shows the RGA measurements with the Argon leak open.

Also put the Full Range Gauge #2 [RGA line] back onto the system to measure the pressure and got a reading of 2.78 E-7 Torr. We believe it is actually lower as the chamber temp is still at 28 degC rather than the 24 it was previously measured at. The gauge also may have needed more time to equilibrate.

  144   Tue Jul 4 15:35:38 2023 PamellaUpdateFLIRFLIR - reflexion problem
[Pamella] I was testing all the positions we need to cover when moving the FLIR camera or the reflector. I tried to find out more about the problem so I tested the position without the mask, just with the old bridge and I got the same problems, in the middle of the screen we have a very good image but if we move we have the visualization problem and we don't see the reflection very well (intensity, emissivity) in FLIR. For this test I used very low current (0.04 A) for keep everything safety. I also think that problem is not in the focal point of the reflector because we can see very well in the center of the screen, but maybe it is because in the parabolic reflector the reflection in the focal point is "extremely" straight, so for you to see the reflection in this point you need keep close to the middle of the screen, to see around the reflector, at the extremes, we need to change the position for the cable or the light to "change" how the flashes of light reflect and thus achieve exactly the position on the camera. It is something like the sketch/ photo attached below.
  143   Mon Jul 3 18:38:13 2023 PamellaUpdateFLIRFLIR project
[Pamella]
  • I was able to work on the python code to do analysis on the FLIR-Reflector data.
  • I could plot images of total area (Tyler help me on that) with csv file and also could have isolation area for triangles. I have attached examples below. Just for now the images are of different data, so there are some differences in the shapes.
  • I'm working on getting a complete analysis code to work with the different positions of the triangles and to be able to do out the statistical analysis.
  • Also we keeping have problem to get good data if when we move the camera or the reflector on horizontal or vertical position. I am working a some ideas for that.
  142   Mon Jul 3 16:26:21 2023 CaoInfrastructureDAQAccess and control Red Pitaya remotely and run it on local machine
[Cao]

To access and control the Red Pitaya using Python locally on a machine within the local network, one should follow these steps:

  1. Start the SCPI server. This is achieved by first log onto the Red Piatay page

    rp-xxxxxx.local/ 
  2. Go to Development >> SCPI server and turn the server on. (Note : The server is currently running)
  3. Communication with Red Piataya is done through PyVista, install PyVista with:
     sudo pip3 install pyvisa pyvisa-py 
    This has been installed on Chimay. Ensure that you have pip3 install, if not, you can install it using:
     sudo apt-install python3 pip 
  4. To start talking to the RedPitaya, ensure you have the scipt
     redpitaya_scpi.py 
    in your local folder. This is the standard class that you will import to your code to establish connection with the Red Pitaya. This code can be found in directory
     ~/RedPiatya 
     or this link
    

  141   Mon Jul 3 14:32:24 2023 CaoInfrastructureVACCooling down vacuum chamber
[Cao]

After leaving the the chamber to bake at 120 deg C from Thursday 3:41 pm. Today I started to cool the chamber down to room temperature at 11:30 am (total bake duration: 91 hours 49 minutes). Ideally, this process should be ramped down slowly, approx. 6 degree per hour. However we had no ramping function with out controller. The only method to tune this cool/ heat rate is to tune the PID parameters, which are:

  1. Pb : Proportional band, this quantity is inversely proportional to the P-gain
  2. ti : Integral time. Increasing integral time makes the output response slower to error, thus the opposite effect of increasing integration gain
  3. td : Differential time
Since the differential term doesn't contribute to rise time significantly, we neglect it for now and first change Pb and ti . The factory default settings :
  1. Pb : 50
  2. ti : 100 s
  3. td : 25 s
Initially Ichanged Pb from 50 to 200 (max) and ti to 999 s (max) but there is a large offset error. Currently, Pb and ti are sitting on the following settings:
  1. Pb : 200
  2. ti : 800 s

At this setting it takes 25-30 mins to drop 6 degrees, which is not as slow as we want but we will have to tune our PID more carefully. At the first stage, I dropped the temperature to 60 deg C. After 3 hours, we dropped the setpoint to 25 degrees and let the vacuum chamber to cool to room temperature.
  140   Fri Jun 30 16:43:14 2023 PamellaUpdateFLIRUpdates: Small moving the FLIR camera
[Pamella]
    Today, I was able to make some adjustments to the FLIR camera angle, suggested by Dr. Richardson, and we got small possible movements keeping the same pattern in the shapes of the triangles. I have attached photos below. I was able to move left and right as well as up and down and it worked in four points that I marked on the table.
    The only problem is that it only worked on a part of the screen, if I try to place it farther to the right or to the left, we are back to the same problem as yesterday.
  139   Fri Jun 30 15:57:28 2023 PamellaUpdateFLIRData and python code update
    [Pamella]
    Updates: Problems with the emission intensity and python code.
  • Yesterday I was working on get data from FLIR reflector but unfortunately we got some problems:
    1. I realized than if I move the reflector a to left or right the screen doesn't get data very well(I attached a photo below). This is a problem because our idea is have the same type of emission every part on screen. Tyler and I worked to tried fix that but don't had success.
    2. Dr. Richardson gave me the idea to move the FLIR camera to left or right (The same happens if I move up and down) and keep the refletor on the same position every time but unfortunately we got the same problem, the screen doesn't get data very well(I attached a photo below). Now I am working to tried fix that.
  • Also I was able to work on the code to isolate the triangle shape for analyzes, I attached the image for that below.
  138   Thu Jun 29 18:27:26 2023 Jon, CaoInfrastructureVACVacuum bake attempt 3: success!
[Jon, Cao]

Summary : We resolved problems with heaters tripping power and were able to proceed with chamber baking

1. Circuit connection adjustment

After yesterday elog 137, today we resolved most of these issues. After Jon contacted Facilities, the LP3B 6 circuit was reset and the cleanroom filter & light panels resumed to work as normal.

Regarding the connection of the heaters. we made the following adjustments:

  • High-temperature controller powering lid + upper volume heater: connect to LP3B 8 circuit (clean room sides, 2 outlets)
  • High-temperature controller powering bottom + lower volume heater : connect to LP3B 4 circuit (workstation side, 2 outlets)

2. Replacement of vacuum nipple insulation

We had also received new insulation pieces from Worbo today to replace the existing insulation with the new ones (see images). These cover the 2 4" tubes (for 6" flanges ) and the 4 1.5" tubes (for 2.75" flanges). The new insulations fit perfectly on these tubes. I also placed all insulation taken off from the last elog back onto the chamber ( these are insulations for the pumps and RGA lines).

3. Baking

We started ramping up chamber temperature at 1:41 pm over the course of two hours:
  • Starting set point: 40 deg C
  • Step increase: 10 deg C up to 80 deg C, 5 deg C from 80 deg to 120 deg C
  • At each step, the temperature readouts show approx. 2.1 deg C overshooting, wait to settle back to approx 1.5 deg C overshoot before increase the set point again
We noticed some smoke emanating from flexible bypass line insulation but none from other locations that were previously smoking . We think this is because the high winding density around the bypass line for such a small volume. Adjustment for next bake: Change the location of PID controller RTD to the bypass line . For now, we remove the insulation around bypass to prevent insulation overheating and encourage convection cooling (see image)

The temperature of the chamber reached as stable 120 deg C without any power issues at 3:45 pm. I waited another 15 minutes to verify its stability and the official baking duration started at 4:00 pm Jun 29 2023. Since we are baking at 120 deg C instead of the standard 150 deg C for Aluminium, the duration for the bake will be over three days until Monday morning, upon which we will slowly ramp down the the temperature.

  137   Wed Jun 28 15:58:56 2023 Shane, CaoInfrastructureVACPower trip problem remains, source of smoke is insulation
[Shane, Cao]

With the new change in wiring configuration described in elog 136, we tried to power up the heaters for baking the vacuum chamber again.

Given that we were worried about the turbo pump overheats, we set the setpoints of of bother high temperature controller and PID controller to be 120 deg C before turning the heaters on

1. Evidence of smoke originating from CoolSkin insulation

We then removed most of the CoolSkin insulation on the Pump and RGA lines ( apart from the one around the flexible bypass line connecting the two ) (see image Pumpline_afterRemoveInsul and RGAline_afterRemoeInsul) . Upon removal of the insulation, we noticed that the insulating foam melted onto the heating tape (see image MeltedInsulation1 and MeltedInsulation2). This is the first indication that the smoke had most likely coming from the insulating foam itself

Once we started baking, upon reaching 80 degree range. We observed no smoke at the location that we removed the insulation. However, We observed smoked coming from underneath the insulation around the flexible pipe, and not from the velcro areas.

What could be causing this, given that the maximum operating temperature of the insulation is 200 deg C? Most likely, the heating tape is much hotter than we think it is. But given that the temperature sensor readout is much lower than 200 deg C, it's likely that this is due to poor thermal contact and it takes a while for sensor to reach a thermal equilibrium with the heating tape. Here, I suggest we should implement the following:
  • We should look into usingsome form of thermal tape (if possible to secure the temperature sensors)
  • Unfortunately or controller does not allow programming process, we will have to implement manual temperature stepping, emulating ramping process over the first hour, until slowly reach 120 deg C
  • OR Tune the PID controller coeffs, especially P and I for longer rise time and settling time

2. The heaters still trip our power

Upon reaching 80 deg C,our main power trip. Unfortunately I don't know how to reset this. Do we need to contact facility on this? Reading elog 136, I noticed that both controllers are connected to the same circuit LP3B 6, which is the same circuit the some of the fan-filters and LED light panels of the cleanroom connected to. From the elog, the circuit has a 20 A limit . An max operation, the 2 heater controllers draw 30 Amps, approx 7 Amps for the fan-filters, and another 1.5 A for LED panel. The combination of these equipment must have overload the circuit and tripped it . Currently half the fans + lights are off in the cleanroom are off due to power trip. Here, I would make a suggestion that each heater controller should be connected to a separate circuit . Currently we LP3B 7 (same side next to LB3B 6) and LB3B 4 (opposite side of the rail) having no equipemts connected to them, but will require cable extensions.
  136   Tue Jun 27 21:47:56 2023 JonInfrastructureVACVacuum chamber bake attempt 1

The electrical overload problem encountered in ELOG 130 has been resolved. The two heater controllers, which draw up to 14.1 A each, overloaded the UPS and tripped one of its circuit breakers, shutting off power to both power strips mounted above the optical table.

I reset the circuit breaker and rerouted the two heater power cables instead to two separate 20 A outlets in the overhead cable tray outside the cleanroom (both on the LP3B 6 circuit). The two high-limit temperature controllers are now permanently positioned, as shown in the photos. For now, the PID controllers have been left sitting at the table level. I am ordering extension cords that will enable us to move those up to the overhead shelf, as well. I ran the heaters in their new configuration for several minutes without issue. Thus we should be able to now proceed with baking the chamber.

For future clarity, I added labels to power strips around the lab indicating which ones are powered by the UPS. To avoid overloading the UPS, only sensitive electronics or devices that could be damaged by a sudden loss of power should be connected to these.

  135   Tue Jun 27 15:18:26 2023 PamellaUpdateFLIRNew data collection
    [Pamella]
    Yesterday, I did a new data collection. I could get a better data in this time and I realized than I need use some angle on the reflector for got a better shot. I need do that because the FLIR camera just is able to get the triangle shape for complete if I keep exactly in same line for center point on the camera but for the data now I need move the refletor to go up and go down. So wasn't working very well if I keep the reflector without angle.
    Now I am using the refletor with a angle. In the more high part I turn the mask for look the table and in the lower part I turn the mask to look up. I attached a photo below for this configuration. Also the processes to get the data was the same than I using last time, the only diference is now I just moved the pillar after get data for high position and lower position for the same reference point on the triangle shape.
    Note: In most data it is impossible to keep the same parameter for current, voltage and temperature. Most have a small variation but not a big difference. For example: I got the temperature in the first position 46.8 °C and in the second position I got 47.1 °C, it's just an example. It's just so we know that we don't have the exact same parameters all the time. In my opinion this is not a problem because it is just a small variation.
    The process to get data
  • 09:35 am: Turned on the device (current on). I wanted for 30 minutes before start get data.
  • 10:05 am: Started taking snap on position one (Reference point: -0.10, 0.050). Parameters:0.11A,1.7V,46.8°C
  • I took four snap on the same position for compare after on data analyzes. I just wanted one minute break between the snaps. I did the same for every position.
  • 10:15 am: Started taking snap on position two (Reference point:-0.10,-0.050 ). Parameters: 0.11A,1.7V,47.1° C
  • 10:22 am: Started taking snap on position three (Reference point:0.00 ,0.050). Parameters: 0.11A,1.6V,48.1°C
  • 10:26 am: Started taking snap on position four (Reference point: 0.00,-0.050). Parameters:0.11A,1.6V,48 °C
  • 10:32 am: Started taking snap on position five (Reference point: 0.05,-0.050). Parameters:0.11A, 1.6V, 48°C
  • 10:37 am: Started taking snap on position six (Reference point: 0.05,0.050). Parameters: 0.11A,1.7V,47.6 °C
  • We can see in the photos attached below every position also I am working in the analyzes.
  134   Tue Jun 27 14:04:42 2023 Sophia A. UpdateMeasuring Noise in InterferometerInterferometer set up and connection to red pitaya
Today we (Sophia and Tyler) constructed the set-up for the electrical noise calculation that I will be conducting this summer. I have included images of the setup below. Our system is effectively a green laser, that feeds into a type of polarizer, then into a beam splitter which sends the laser light down two arms into detectors. We started by connecting the detectors to an oscilloscope to determine whether the signal will exceed 1V, as the red pitaya (our planned data collection device) cannot receive signals with a higher voltage than 1V. We spent most of our time calibrating the oscilloscope and fine-tuning the set-up so that we would have approximately equal voltages in each arm of the interferometer. Once confirming that the output voltage would not meet or exceed 1V, we switched from an oscilloscope to the red pitaya for our measurements. Now that the system is set up, we will be able to run code in the red pitaya interface that will run an FFT on the signal, and then do noise analysis from there.
  133   Tue Jun 27 12:09:37 2023 ShaneUpdateCleanroomcleanroom 5 zone particle count measurement
Attached is 5 zone measurement for cleanroom particulate count. Zone 3 (in front of vacuum chamber) higher than usual, likely due to recent vac work. Slightly above ISO class 5 standard in 1.0 micron range, measuring 997 particles/cubic meter while ISO standard is 832 particles/cubic meter in this range. Zero count test on particle counter performed prior to today's measurement.
  132   Fri Jun 23 15:47:06 2023 PamellaUpdateFLIRCollecting data - Moving horizontal and vertical on screen.
[Pamella]
  • 02:09 pm: Turned on the device (current on)
  • 02:42 pm: Started taking snap on position one (Reference point: 0,-0.062). Parameters:0.10A,1.5V,41.5C
  • I took multiplier snap on the same position for compare after on data analyzes. I just wanted one/two minute break between the snaps. I did that same for every position.
  • 02:55 pm: Started taking snap on position two (Reference point:-0.10,-0.062 ). Parameters: 0.10A,1.5v,43 C
  • 03:01 pm: Started taking snap on position three (Reference point:0.05 ,-0.062). Parameters: 0.1A,1.4V,42.8C
  • 03:07 pm: Started taking snap on position four (Reference point: 0.05,0.045). Parameters:0.10A,1.5V,43.6 C
  • 03:15 pm: Started taking snap on position five (Reference point: 0,0.045). Parameters:0.10A, 1.4V, 44.1C
  • 03:22 pm: Started taking snap on position six (Reference point: 0,0.045). Parameters: 0.10A,1.4V,43.3 C
  • We can see in the photos attached below than have some differences between every position so I should be starting analyzes on that.
  131   Thu Jun 22 13:58:00 2023 Pamella, Julian and ShaneUpdateCleanroomCleaning and Particle Count
[Pamella, Shane, and Julian]
    cleaning cleanroom and particle count
  • 12:00 pm: started particle count
    • Zone 3
      • 0.3u: 3533
      • 0.5u: 540
      • 1.0u: 166
    • Zone 4
      • 0.3u: 290
      • 0.5u: 124
      • 1.0u: 41
  • 12:31 pm: Started checking the surface inside the cleanroom and began surface wipedown
  • 12:50 pm: started vacuuming the floor
  • 1:05 pm: Finished vacuuming floor
  • 1:09 pm: Started mopping the floor
  • 1:21 pm: Finished mopping the floor
  • 1:22 pm: Started cleaning the baskets
  • 1:25 pm: Started mopping with IPA wipes
  • 1:39 pm: Finished mopping with IPA wipes
  • 1:41 pm: Changed sticky floor mats
  • 1:45 pm: Started particle count
    • Zone 3
      • 0.3u: 2327
      • 0.5u: 581
      • 1.0u: 207
    • Zone 4
      • 0.3u: 1662
      • 0.5u: 374
      • 1.0u: 290
  130   Wed Jun 21 20:25:05 2023 CaoInfrastructureVACVacuum chamber bake attempt 1

TL;DR:

We are not yet able to bake the chamber at 150 deg C due to some current limit, most likely caused power supply switching off. Also, smoke was observed at some insulation points, mainly in the small arm sections, This is likely because the insulation does not fit well and the velcro came into direct contact with heat tape. Some Velcro (made from Nylon/ Polyester) has lower melting temperature point (in 90-120 deg C range)

Full version:

20 June 23:

  • Turn off heater (short term testing) Close valves to RGA line and main volume. Pressure (Torr) readout:
    • Gauge 1 (main volume): 3.43E-6
    • Gauge 2 (RGA line): 2.61E-6
    • Gauge 2 (pump line): 3.8E-4
  • Turn off turbo pump, let vacuum line vent
  • Connect high temperature control unit to main power, power up, set setpoints:
    • Temperature setpoint: 150 deg C
    • High temperature setpoint (to switch off) : 175 deg C
    • Hysteresis: 10 dec C
  • change setpoint of PID control unit to 150 dec C, with high alarm set at 165 deg C
  • Connect power output of high temperature control units to PID temperature control units, ensuring both are off
  • Turn off scroll pump
  • Replace Pirani gauge in front of turbo pump with blanks (see image)
  • Pump the vacuum line back down
  • Open up valves and wait until pressure of full system drop back down to 1E-6
  • Install the high temperature controller thermocouples onto the chamber (see images):
    • One thermocouple is installed on the other side of the cross before the turbo pump
    • One thermocouple is installed on the main volume next to the PID controller RTD
  • Attempt to remove electronic box and magnetic shield of full range gauges:
    • Electronic box is easily removed with an Allen key
    • Magnetic shield cannot be removed since the gap between the vacuum flange and the gauge bolt is too short for a spanner to go in. This is mainly due to the bolt washers are in the way (see images)
    • To remove the magnetic shield, the main volume has to be vented and the gauges need to be readjusted.
  • Attempt to power heaters (but only heat to 80 deg C):
  • Leaving the gauges intact, the high temperature controller + PID controller are turned on to test heating the chamber
  • At this point, both of the high temperature controllers are connected to the same power strip (Vacuum chamber end of the table)
  • After heating up to 65-70 deg C range, the powers turned off on both controllers + the lights on one end of the table
  • Upon inspection, the power strip has turned itself off, I don't know what the model of the power strip but we should check its current limit
  • For a quick test, I connect one of the two heater controlling system to the power board on the work desk while leaving the other running off the same power strip: The heaters appeared to be function ok and able to reach 80 deg C, at which point I turned it off and left for the day

21 June 23:

The goals of today was to remove the electronic boxes and magnetic shields on full range gauges to enable high temperature bakeout

  • Upon returning to the lab, the gauges readout of vacuum pressures were:
    • Gauge 1 (main volume): 3.31E-7
    • Gauge 2 (RGA line): 3.40E-7
  • Venting the both main volume and RGA line
  • Remove the two full range gauges from their flanges
  • Electronic boxes and magnetic shields were removed according to the gauge manuals (see images)
  • Mount the gauges (with only its probing volume) back onto their respective flanges, ensuring that the flange washers do not block access to the magnetic shield screws
  • Only remount magnetic shield + electronic box for one gauge (gauge 2: RGA line) for monitoring chamber pressure
  • Turn on scroll pump and let the chamber pump down
  • Rearrange heater controller connections while waiting for pumping down:
    1. Controllers for bottom + pump & RGA line heaters remain the same: connected to power strip on vacuum end of the table
    2. Controllers for lid + upper chamber main volume: connected to power strip on clean&bake end of the table
  • Once the pressure readout by gauge 2 reached 3 Torr, the turbo pump was turned on and left to run for 45 minutes
  • Upon returning to the lab, pressure on gauge 2 read 5E-6 Torr and was still decreasing
  • Disconnect the ethernet cable to gauge 2, remove its electronic box and magnetic shield
  • Turn on heater controller units and let them drive the heaters to get up 150 deg C
  • At 95 degree range, I could see smoke at some locations, mainly the RGA and pump lines where the insulation do not fit properly and the velcros are likely to be overheated
  • Upon reaching 90 degree range (measured by sensors), the powers turned off on both sides of table (including heaters, lights and scroll pump)
    • Turn off both heaters controllers and unplug them from power strip. Attempt to switch the power strip back on but nothing happened
    • It is now not the power strips problem and must be further down the line from outside the tent, most likely the power supply that these strips connected to: What is the power supply model + current limit?
  • The heater controllers left unplugged, I temporarily plugged scroll pump to the desk power strip so it can still run

  129   Tue Jun 20 22:14:24 2023 Pamella, CaoInfrastructureVACShort term testing of vacuum heater controller units
[Pamella, Cao]

Fuse replacement

  • Replace blown 10A fuse in ucontroller outside cleanroom
  • Replace 10 A fuse in main power connection slot of the controller unit inside cleanroom
  • Pamella wiped down unit outside cleanroom.
  • Controller units turned on and temperature setpoint set to be 80 deg C
  • Temperature settle in approx. 15 minutes(as recorded by the RTD). No problems with fuses observed
  • Recording of pressure gauges (in Torr) :
    1. Before turning heater on :
      1. Gauge 1(main chamber): 3.73E-7
      2. Gauge 2(RGA line): 3.65E-7
      3. Gauge 3(Pump line): 3.8E-4
    2. After 15 minutes :
      1. Gauge 1(main chamber): 7.07E-7
      2. Gauge 2(RGA line): 6.12E-7
      3. Gauge 3(Pump line): 3.8E-4
  • Reduce setpoint temperature to 60 deg C due to Pinrani gauge (Gauge 3) temperature limit
  • Upon returned to lab to reduce temperature (35 minutes after turned on):
    1. Gauge 1(main chamber): 1.22E-6
    2. Gauge 2(RGA line): 9.98E-7
    3. Gauge 3(Pump line): 3.8E-4
  • Once temperature has settled to 60 C (approx 20 mins after changing setpoint), pressure readout showed:
    1. Gauge 1(main chamber): 1.37E-6
    2. Gauge 2(RGA line): 1.10E-6
    3. Gauge 3(Pump line): 3.8E-4
  • Heater left on for the whole afternoon, pressure readout upon returning to lab at 5:30 pm:
    1. Gauge 1(main chamber): 3.43E-6
    2. Gauge 2(RGA line): 2.61E-6
    3. Gauge 3(Pump line): 3.8E-4

  128   Tue Jun 20 17:28:23 2023 PamellaUpdateElectronicsHeater system parts - Wiped
[Pamella]
    Heating system
    Wiping the heater system parts.
  • 04:37 pm: Started wiping the electronic device part for the heater system (HL101 Series Digital Benchtop temperature limit control).
  • 05:19 pm: Finished wiping the parts to the heater system (HL101 Series Digital Benchtop temperature limit control). I wiped the HL101 Series Digital Benchtop temperature limit control and I didn't bagged and tagged because we should install that soon.
  • 05:23 pm: I putted heater electronic device inside the cleanroom without the bag. Also the electronic device is near to the vacuum chamber and the other parts to heater system.
  • I attached the photo below.
  127   Mon Jun 19 11:20:57 2023 PamellaUpdateFLIRFLIR - Fixed some problems
[Pamella]
  • 08:59 am: Turned on the electronic device (current on) for started taking data.
  • 09:37 am: Tried understanding the error in the focal point. I realized the pillars was in the wrong place and because of that we got problems to keep the reflector in the correct position to FLIR focus.
  • 09:58 am: Started checking the temperature and the parameters.Changed the pillars to the original position (0.5645m) just for checking with the problem was the pillar in the wrong place.
  • 10:06 am: Changed the reflector to point (0.3282m) and now in the correct position for the pillars. Started take snap and collecting data. I moved up and down the reflector for got data to compare later.
  • 10:37 am: Used the closest point possible for the reflector in front of the FLIR camera with the correct spot for the pillars.(0.2032m)
  • 11:00 am: Started taking snap after kept the current on for a few hours. Parameters: Current: 0.10A , Volt: 1.3V and Temperature: 41.9 C.
  • I attached below the snap in the most close point possible, now i can see a better photo and I think a fixed the problem about the focal point in the reflector for have more uniformity between the triangles, isn't perfect yet but now is just some adjustments. Furthermore after that I should be change the reflector position and also the optical focus distance in the FLIR camera and try use the black wall.
      126   Fri Jun 16 17:40:28 2023 AidenUpdateClean & BakeClean and Bake Batch 14
    Cleaned and Baked the new and 2.75" copper gaskets for the vacuum system. Cleaned them with liquinox in the ultra sonic washer for 10 minutes. Then dried them with nitrogen. Then put the copper parts into the oven for the following steps; 1. Ramp to 100 degC in 15 minutes 2. Dwell at 100 degC for 30 minutes 3. Ramp to 175 degC in 30 minutes 4. Dwell at 175 degC for 24 hours 5. Turn off Also bagged and tagged the parts from Batch 13 and placed them into the clean room on the computer table.
      125   Fri Jun 16 16:17:13 2023 PamellaUpdateFLIRFLIR - Change the position
    [Pamella]
      Today I change the distance between the FLIR camera and reflector (3D-Mask with mirrors and light). Now the distance is 0.3282 m.
    • Note: In this distance is possible move up and down the reflector and take data to compare.
    • The focal point inside the reflector keeping like little problem, every time I tried adjust this I got some triangles is not with "perfect emission" (looks like different than the others). Also if I move up or down the focal point inside the reflector have some issues as well.Therefore I am working on that.
      124   Wed Jun 14 15:35:36 2023 PamellaUpdateVACHeating system installation
    [Pamella and Cao]
      Heating system installation - Second day.
    • Today we kept installing the equipment for the heating system.
    • First: Started installing the two heating cable around the chamber vacuum, the arms and covered it with aluminum tape.
    • Second: Started installing the insulation stuff around the vacuum chamber and around the connections points (the arms) in the vacuum chamber.
    • Third:Started installing the heater system (electronic device) and tried testing.
      • Note: The around part of the chamber vacuum was difficult to cover, so we spent a little time on. Also one heater system electronic device wasn't working because one fuse is burned so we could not finished this part and we need wait for a new one to replace and working on it.
      123   Tue Jun 13 21:33:46 2023 PamellaUpdateGeneralNew cabinet for PPI
    [Pamella and Dr.Richardson]
      Dr. Richardson installed the new cabinet outside the room for the PPI equipments, and then I wiped all surfaces inside and outside of the new cabinet.
      Dr.Richardson and I have finished organizing the PPI within the new cabinet. Also we have new supplies of gloves, and will likely have more supplies for other PPIs soon.
      122   Tue Jun 13 21:08:46 2023 PamellaInfrastructureVACHeater system - Installation
    [Pamella, Cao and Jon]
      Heating system installation
    • Today we started installing the equipments for the heating system.
    • First: Started installing the heating cable on the top lid and covered it with aluminum tape.
    • Second: Started installing the insulation cover on top of the chamber lid.
    • Third:Started installing the heating cable from under the vacuum chamber and covered with aluminum tape.
    • Forth: Started installing the insulation cover under the vacuum chamber
    • Note: The under part of the chamber vacuum was very difficult to cover, so we spent a little time on it and we couldn't finish the whole installation today. So tomorrow we should be able to keep doing the installation.
      121   Tue Jun 13 13:25:05 2023 AidenSummaryClean & BakeClean and Bake Batch 13
    Cleaned and Baked the new 1.33" and 2.75" blanks for the vacuum system. Cleaned them with liquinox in the ultra sonic washer for 10 minutes. Then dried them with nitrogen. Then put the two stainless steel parts into the oven for the following steps; 1. Ramp to 100 degC in 15 minutes 2. Dwell at 100 degC for 30 minutes 3. Ramp to 200 degC in 30 minutes 4. Dwell at 200 degC for 48 hours 5. Turn off
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