cleaning cleanroom and particle count

• 5:10 pm: ran zero count test on particle counter
• 5:14 pm: started particle count

  NOTE: initial counts are significantly above allowed limit. ~10 times larger than ISO class 5 standard in the smallest size range. Realized partway through ceiling tile changes that the power/lights for some of the hepa fans in the ceiling frame had been turned off. May explain this high number. Have since turned fans back back on.

  • zone 3:
    • 0.3 u: 109208
    • 0.5 u: 16337
    • 1.0 u: 581
• zone 4:
  • 0.3 u: 51340
  • 0.5 u: 9228
  • 1.0 u: 581
• 5:33 pm: started replacing ceiling tiles
• 6:25 pm: began surface check and wipedown, including softwalls
• 6:33 pm: started vacuuming the floor
• 6:45 pm: finished vacuuming the floor
• 6:45 pm: started mopping the floor
• 6:50 pm: finished mopping the floor
• 6:52 pm: started cleaning the buckets
• 6:53 pm: started mopping with IPA wipes
• 6:58 pm: finished mopping with IPA wipes
• 6:59 pm: changed sticky floor mats
• 7:00 pm: started particle count
  • zone 3:
    • 0.3 u: 5404
    • 0.5 u: 1413
    • 1.0 u: 41
• zone 4:
  • 0.3 u: 1704
  • 0.5 u: 332
  • 1.0 u: 166

Summary

Today I finished implementing an RTS model to read out the integrated FROSTI RTDs (temperature sensors) via the CyMAC. The model is named "MSC" and is located at cymac:/opt/rtcds/usercode/models/c1msc.mdl. We successfully tested it with the heater elements operating in vacuum at low power (12 VDC), finding them to reach an average steady-state temperature of 160 C.

From the cymac host, the MEDM control screen can be accessed with the terminal command "sitemap" (from any directory).

Measurement Technique

Each FROSTI heater element [299] contains an internal two-wire RTD placed near the front emitting surface, which enables the temperature of the blackbody emitter to be directly monitored. From the measured temperature and the emissivity of the uncoated aluminum nitride surface (known to be ~1 in the IR), the radiated source-plane power can also be estimated.

The resistance of each RTD is measured via a ratiometric technique. The RTDs are powered in series with a 1 kΩ reference resistor located inside the readout chassis [305], whose temperature is not changing. The signal is obtained by taking the ratio of the voltage difference across each individual RTD to the voltage difference across the reference resisitor. The advantage of this technique is that the ratio of  the voltage differences is insensitive to changes in the current through the resistors (since they are all in series; see [271] for wiring diagram).

Implementation Detail

The signal flow is shown in Attachment 1. The eight RTD signals enter through ADC channels 0-7, along with the reference resistor signal on channel 8. The first set of filter modules apply a calibration gain to convert the signals from raw ADU counts to units of input-referred voltage. The ratio of each RTD signal to the reference resistor signal is then taken. The second set of filter modules multiply the voltage-difference ratios by the resistance of the reference resistor, 1 kΩ ± 0.01%, to obtain the RTD resistances in physical units of ohms.

Finally, a freeform math module is used to invert the quadratic relation between each RTD's resistance and temperature. The final signals passed to the third set of filter modules are the RTD temperatures in physical units of degrees C. The temperatures of the tungsten RTDs are estimated assuming TCR coefficients of A=0.0030 C^-1 (±10%) and B=1.003E-6 C^-2, which were provided by the manufacturer.

One DAC channel is used to provide the excitation voltage for the RTD measurement, which is visible on the far right of the control screen. At its maximum output voltage of +10 V, the DAC can drive a maximum current of 10 mA.

After further modification of the RTD readout chassis (i.e. adding resistors, placing reference resistor in front of RTDs), here are the following direct measurements:

RTD 1: 0.484 V

RTD 2: 0.486 V

RTD 3: 0.503 V

RTD 4: 0.474 V

RTD 5: 0.495 V

RTD 6: 0.483 V

RTD 7: 0.476 V

RTD 8: 0.510 V

Reference: 5.847 V

Here are the Cymac signal readings:

RTD 1: 74

RTD 2: 67

RTD 3: 73

RTD 4: 45

RTD 5: 82

RTD 6: 75

RTD 7: 70

RTD 8: 71

Reference: 884

The one (possible) discrepancy here is the readout for RTD 4 via Cymac, since it's signal reading is ~30 counts lower than the others. I do not believe this is a wiring issue due to the direct measurements taken.

After updating the wiring in the RTD Chassis, a signal is now seen at each ADC input. However, there seems to be a discrepancy between the voltages I measured out with the multimeter (see below). Next steps include:

• Finish final debugging
• Calibrate ADC inputs with known voltage source (likely to use DAC).

Voltage Readings:

RTD 1: 0.576 V

RTD 2: 0.578 V

RTD 3: 0.598 V

RTD 4: 0.563 V

RTD 5: 0.477 V

RTD 6: 0.463 V

RTD 7: 0.456 V

RTD 8: 0.491 V

Reference Resistor: 5.463 V

Total Voltage: 9.665 V

Took more data today and the chamber and elements are showing an even lower HC level than we have gotten before. It is safe to say that the elements are not contaminated and out gassing HC into the chamber.

Heater 1= 73.6; 81.8

Heater 2= 70.4; 82.1

Heater 3= 71; 84.5

Heater 4= 71.5; 80

Heater 5= 70.5; 81.7

Heater 6= 72; 79.4

Heater 7= 69.2; 78.2

Heater 8= 71.1; 84.2

Below is the data for the most recent bake. I believe the chamber is cleaner than it is actually showing as the RGA data was still getting lower while the data was being taken. I will take the data again tomorrow just in case. Still, the data shows that the chamber is basically as clean as it was before bake 10 and this means further power testing can proceed.

Helium leak tested the chamber again today to check if the sealant changed anything. The two primary target flanges from last time have improved significantly with the flange from the RGA on the cross now being below 2e-14. While the turbo pump flange was leaking at a rate of 4e-13. Much better than what it has been before.

I performed another continuity test on the RTD chassis wiring, and everything seems to be set up correctly. The chassis should be ready for installation.

[Jon, Tyler, Aiden, Shane, Pooyan, Michael, Cynthia, Luke]

On Wednesday, we completed long list of work towards making the new lab (1129) fully operational and enabling the next phase of FROSTI testing. 

Cabinet Installation

Three new VWR cabinets with sliding glass doors were installed in 1129. Each unit measures 48" (W) x 22" (D) x 84" (H) and sits along the back wall (see attachment 1). The 350-lb. cabinets were laid in place by Facilities on Monday and permanentized on Wednesday. Work included:

• Earthquake anchoring to the masonry wall
• Sliding glass doors leveled
• Shelving installed
• Wiping down of interior and exterior surfaces with IPA wipes

Server Rack Installation

A new Tripp Lite 42U open-frame rack was laid in place in 1129 and anchored to the floor (see attachment 1). This rack will house all of our general-purpose and simulation computers, which will be relocated from the 1119 rack at a later time.

Lab Clean-Up

Following installation of the new cabinets and rack, we proceeded to organize and clean both labs. Work included:

• Moved parts and equipment into permanent storage in 1129 cabinets
• Wiped down surfaces in 1119 and 1129 with polypropylene IPA wipes
• HEPA-vacuumed floors of 1119 and 1129
• Mopped floor in 1119 with Liquinox solution
• Installed new sticky mats in 1119 and 1129
• Regular cleanroom cleaning and particle counts (see 302)
• Positioned new stainless steel gowning bench outside the cleanroom (see attachment 2)

At this point, the only piece of lab equipment still to be delivered is a HEPA garment cabinet for reusing our (semi-disposable) bunny suits. It is schedule to arrive in mid-February and will sit outside the cleanroom in 1119, in the former location of the HEPA flow bench.

cleaning cleanroom and particle count

• 2:03 pm: changed sticky floor mats
• 2:05 pm: started particle count
  • zone 3:
    • 0.3 u: 4863
    • 0.5 u: 1205
    • 1.0 u: 872
• zone 4:
  • 0.3 u: 1953
  • 0.5 u: 789
  • 1.0 u: 457
• 2:35 pm: began surface check and wipedown, including softwalls and ceiling tiles
• 2:45 pm: started vacuuming the floor
• 2:56 pm: finished vacuuming the floor
• 2:57 pm: started mopping the floor
• 3:01 pm: finished mopping the floor
• 3:02 pm: started cleaning the buckets
• 3:05 pm: started mopping with IPA wipes
• 3:08 pm: finished mopping with IPA wipes
• 3:09 pm: started particle count
  • zone 3:
    • 0.3 u: 5528
    • 0.5 u: 2203
    • 1.0 u: 1662
• zone 4:
  • 0.3 u: 1080
  • 0.5 u: 415
  • 1.0 u: 332

Leak tested each flange and weld and only found two flanges to have noticeable leaks with the electron multiplier on. These were the turbo pump flange and the RGA flange that connects to the cross. The RGA one is rather new as it has not had a measurable leak before and it was around 2 e-8. We then applied the new sealant to these two flanges as directed by the instructions on the packaging.

Then after waiting a few minutes for the sealant to dry we started the bake. We got the PID controllers set to 120 after many steps and we checked the temperature of the flanges throughout this increase. The flanges never reached 70C with the electronics still left on it. The RGA was left on as well.

Below is the current state of the RTD readout chassis wiring. Initial continuity tests seem good, will run through one more time to confirm.

Installed the heater elements into their fixture and prepped the cables by twisting the wires into pairs. We also installed the pins onto the wires and placed them into the peek DB 25 connector. The installation tool we had did not fit the pin size we had so the pins needed to be installed by hand by opening the connector and holding them in place. In the future we will need to make sure we twist the wires together, group them, and then splice them all to the same size for easier installation. We then grouped all the twisted pairs into a bundle and zipped them together. On the left with two peek zip ties is the power and on the right is the RTD with one peek zip tie. This orientation remains true when looking at the feed through flange from the outside with the power port on closest to the wall.

We also installed the heater elements numbered 1-8 starting from the left in image 3. These elements have numbers as resistance data was taken before as to identify the heaters after they are in the chamber. After installing the DB 25 connectors we tested that the pins were in the right orientation by using a volt meter and testing the resistance where the cable runs into the the actual power supply. It seems that all the pins were properly installed and the resistance values all match with each one gaining about 2 Ohms from the cable itself.

Then the pump down was started. The pump was very slow and we suspected a leak but after changing the o-ring pump down was not any faster and we decided to leave it over break as it seemed to just be water outgassing from the aluminum. The chamber is now able to be RGA scanned and leak tested before the next bake as it is low enough pressure.

The custom front and rear panels for the RTD readout chassis arrived last Friday. I installed them in the chassis frame to check their fit. They fit very well, so all that now remains is to complete the internal wiring and test the connections.

The chassis panel designs are archived to LIGO-D2300452 and LIGO-D2300453.

Update: I have completed permanent routing of the electrical cables. I also ran the ultrasonic washer's drain line to the sink drain (the current hose does reach). The new clean and bake lab is now fully operational.

[Jon, Tyler, Aiden, Luke]

On Friday we completed assembly of the new stainless steel-topped benches in 1129. We then moved the clean and bake equipment from 1119 to its new larger space in 1129. This included the HEPA flow bench, ultrasonic washer, deionized water drum, nitrogen tanks, and forced-convection oven. The oven was re-anchored to the wall with earthquake restraints in its new location.

The power cords still need to be permanently routed, but the new clean and bake lab is otherwise ready for use.

I measured the temperature of the flanges where some of the electronics will go and I found that the RGA flange was at 55C and the two full range gauges were at 65C. I also stopped bake 9 to cool down for measurement.

1. Turn off the RGA filament and disconnect it.

2. Record the pressure and then close the angle valve and gate valve on the RGA line to isolate it from the system.

3. Turn off the backing and turbo pump and let the turbo pump spin to a stop by slowly leaking the chamber. The slower the safer.

4.Slowly open the vents on the chamber and the turbo pump. Making sure not to raise the pressure too fast.

5. Once done venting the chamber, open the lid by removing the bolts and prying the lid open with a long flat head screw driver.

6. Removed previous parts and placed them into clean bags. Place new parts inside of the chamber and group them together close to the center.

7. Place the lid back onto the chamber and tighten the bolts in a circular pattern until tightened all the way with the wrench.

8. Make sure all vents are closed and turn the backing pump back on.

9. The turbo pump can be turned back on when the pressure reaches e-1 torr.

10. Wait until the chamber reaches a pressure of e-6 torr before opening the angle and gate valve on the RGA line. After the RGA line is open and the pressure is still below e-6 torr, the RGA filament can be turned on and a leak test of the lid should be performed.

11. After the leak test shows no leaks, proceed with starting the low temp bake.

Below is the procedure we will follow to assemble the FROSTI prototype.

1. Install SS guide rods and bottom Macor spacers in bottom reflector
2. Install AlN elements on top of bottom Macor spacers
3. Install upper Macor spacers on top of AlN elements
4. Feed unterminated power and RTD leads through slots in upper reflector
5. Install upper reflector, using guide rods to slowly lower into position
6. Install vented SS bolts for reflectors; Macor bolts for heater elements
7. Remove SS guide rods
8. Bundle power and sensing cable with PEEK cable ties and SS cable mounts
9. Terminate power and sensing cable bundles with PEEK DB25M connectors

[Jon, Tyler, Shane, Luis]

On Wednesday we completed the migration of the electronics workshop from 1119 to the large new workbenches in 1129. The two workstations pictured closest to the front of the room are for electronics assembly and testing, while the two in the rear will house LIGO CDS workstations. We moved all of the tools, cabling, and soldering and test equipment from 1119 to this new location. We also moved the large tool chest to 1129, as pictured, and moved the smaller tool chest to 1119 in its place.

The electronics workbench is ready for use. 

cleaning cleanroom and particle count

• 12:30 pm: ran zero count test on particle counter
• 12:32 pm: started particle count.
  • zone 3:
    • 0.3 u: 59,488
    • 0.5 u: 9561
    • 1.0 u: 706
• zone 4:
  • 0.3 u: 7732
  • 0.5 u: 1912
  • 1.0 u: 290

NOTE: Frame ceiling tile collapsed in cleanroom, explaining insanely high 0.3 u particle count in zone 3 (nearly 6 times above limit). Wiped down tile and put it back in ceiling frame.

• 12:56 pm: began surface check and wipedown, including softwalls
• 1:16 pm: started vacuuming the floor
• 1:32 pm: finished vacuuming the floor
• 1:33 pm: started mopping the floor
• 1:47 pm: finished mopping the floor
• 1:48 pm: started cleaning the buckets
• 1:53 pm: started mopping with IPA wipes
• 2:05 pm: finished mopping with IPA wipes
• 2:06 pm: changed sticky floor mats
• 1:53 pm: started particle count
  • zone 3:
    • 0.3 u: 6401
    • 0.5 u: 3450
    • 1.0 u: 1787
• zone 4:
  • 0.3 u: 4073
  • 0.5 u: 2452
  • 1.0 u: 1039

Took some RGA data of the chamber after it has been cooling down. I do not believe that this data accurately shows the HC levels in the chamber as the pressure is still above where it was at before the bake and was still falling. I believe more time is needed to let the pressure fall and for the RGA filament to remain on to return to a point where the data can be trusted.

Turned off the heating tape today in anticipation to take more RGA data on Sunday or Monday morning before the meeting.

Came into the lab in the morning to check on the chamber heating. I decided to set the PID controllers to 110C rather than 120C as the chamber lid and wall were reading near 140C. With the PID controllers at 110C the chamber lid and wall now read 126C and 132C. Currently the PID controllers are placed on the cross in front of the RGA and the reducing nipple in front of the turbo pump. I believe this is a good equilibrium and will leave the tape on until Saturday when it will be turned off to cool down.

The workbenches are now completely assembled and put into their final places. Additionally, the tool chest has been moved.

After the bake is done on Saturday it will be cooled down and RGA data will be taken to measure the out gassing rate of the stainless steel fasteners inside the chamber. Then on Tuesday we will plan to vent and open the chamber again to put the macor inside and repeat the another low temp bake and then test the macor early in week 11. Then the next material will be the aluminum mounting hardware for mounting the heaters and that should hopefully be done before the end of week 11 so the heaters can be tested afterwards after being cleaned with vector alpha wipes.

The tabletops have been attached to the workbench frames. Unfortunately, one of the tabletops came out of the box with a large scratch and small dent in the middle. One of the electric top shelves is ready to be attached to the undamaged table, but the other is yet to be opened. Assembly will be completed Wednesday morning.

Update: I was able to put the FROSTI power controller on the lab network. It is connected to the switch in the top of the rack and is assigned a static IP address of 192.168.1.12 and an NDS hostname of relay1.

The controller can be remotely accessed through an SSH command line interface as well as an HTML webpage, which can be opened from any web browser on the lab network by navigating to the above IP address (the login credentials are the same as for the workstation computers).

There is also an unofficial Python package for interfacing with the controller: dlipower. We will investigate using this package to interface the controller with soft EPICS channels hosted on the CyMAC. This will allow us to create a custom MEDM screen for controlling the FROSTI heater elements.

Edit: The login credentials were set up to be the same as for the CDS workstations.

Luis and Aiden vented the chamber today. We closed off the RGA section and then proceeded to open the the vent on the main body after turning off the turbo and backing pump. We then opened the lid and placed in all the stainless steel hardware that will be used in evaluating the FROSTI optics and heater elements. We also inspected the weldments before closing it up. Check the clean and bake data base where there is now a new section outlining the parts in each test. We then closed the lid, tightened the bolts, turned the backing pump back on and let the pressure drop until it was below 1e-1 torr. Then turned the turbo pump back on and after a few hours the pressure was back down to 4.16e-7 torr. The RGA was turned off during all of this and was turned back on when done even though we closed both valves to keep the RGA volume under vacuum.

[Tyler, Shane, Mohak, Cynthia, Luke, Michael, Luis]

[Aiden, Luis]

Tested every weld and flange to find leaks. Only found that the flange on the turbo pump and reducing nipple was still at 2e-9 torr on the leak. The chamber still rose in pressure when the two gate valves were closed but no noticeable leak could be found on the lid or welds.